自然水体和土壤中氯代烃和芳香烃类化合物分析测试方法研究

修回日期: 2007-12-26

刊出日期: 2008-06-28

A Methodological Study on Determination of Chlorinated Hydrocarbons and Aromatics Hydrocarbons in Natural Water and Soil Samples

Revised Date: 26 December 2007

Publish Date: 28 June 2008

摘要: 利用内标物,固相萃取剂和选择离子监测气相色谱-质谱分析方法对自然水体和土壤中氯代烃和芳香烃类化合物进行定量检测.分析结果显示,水样的平均误差基本在25%以内,土壤样品在10%以内,误差随着化合物浓度的降低而增大.方法简化了样品处理程序.
- 固相萃取 /
- 选择性离子监测 /
- 气相色谱-质谱法 /
- 内标 /
- 氯代烃 /
- 芳香烃 /
- 自然水体 /
- 土壤样品 /
- 氯代烃 /
- 芳香烃类化合物 /
- 化合物分析 /
- 测试方法 /
- 研究 /
- Soil /
- Natural /
- Water /
- Hydrocarbons /
- Aromatics /
- Determination /
- 处理程序 /
- 简化 /
- 浓度 /
- 平均误差 /
- 水样 /
- 显示 /
- 结果 /
- 定量检测
Abstract: A method for analysis of chlorinated hydrocarbons and aromatics hydrocarbons in natural water and soil samples by selected ion monitoring GC-MS (SIM) with internal standardization was developed. The analytes in the samples were separated and pre-concentrated by solid phase extraction. The analytical results show that the average errors for the analytes are within 25% in water samples and within 10% in soil samples and the analytical errors enlarge with the decrease of the analyte concentration.
- solid /
- phase /
- extraction； /
- selected /
- ion /
- monitoring； /
- gas /
- chromatographymass /
- spectrometry /
- internal /
- standard /
- chlorinated /
- hydrocarbons； /
- aromatic /
- hydrocarbons /