空气滤膜采集大气浮尘样品中多元素的测定

收稿日期: 2008-11-01

修回日期: 2008-12-29

刊出日期: 2009-10-28

Determination of Multi-elements in Airborne Dust with Air Filtrer Membrance Sampling

Received Date: 01 November 2008

Revised Date: 29 December 2008

Publish Date: 28 October 2009

摘要: 用氢氟酸-盐酸-硝酸-高氯酸体系对空气滤膜上附着的浮尘样品进行分解，电感耦合等离子体发射光谱法、电感耦合等离子体质谱法同时测定溶液中15个主量和微量元素铁、铜、锌、镍、镧、铈、锂、锰、铬、镉、钴、铅、钍、铊、铀。将国家一级标准物质模拟浮尘样品加入空白滤膜进行测定，结果与标准值相符。各元素4次测定结果的相对标准偏差（RSD）小于5%。
- 空气滤膜； /
- 电感耦合等离子体发射光谱法； /
- 电感耦合等离子体质谱法； /
- 酸溶； /
- 主量和微量元素； /
- 国家标准物质； /
- 大气浮尘
Abstract: Airborne dust sample was collected with air filtrer membrance and then dissolved with mixed acid of HFHCl-HNO3-HClO4. 15 elements including Fe, Cu, Zn, Ni, La, Ce, Li, Mn, Cr, Cd, Co, Pb, Th, Tl, and U in the sample solution were determined by inductively coupled plasma-atomic emission spectrometry (ICP-AES) and inductively coupled plasmamass spectrometry (ICP-MS). The National Standard Reference Materials, simulated as airborne dust, were collected with air filtrer membrance and analyzed by ICP-AES and ICP-MS. The results were in agreement with the certified values with precision of less than 5%RSD (n=4) for all these elements.
- air /
- filter /
- membrance； /
- inductively /
- coupled /
- plasma-atomic /
- emission