银-二乙基二硫代氨基甲酸钠法测定铁矿石中砷溶样方式的改进
Improvement of Sample Dissolution Method for the Determination of Arsenic in Iron Ores by Ag-DDTC Method
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摘要: 改进了铁矿石样品溶解方法,尝试用硫-磷混酸溶解铁矿石样品,缩短了分析时间,提高了分析精度。溶解后的样品以银-二乙基二硫代氨基甲酸钠法(Ag—DDTC)用于部级标准物质测定,砷的测定结果与标准值相符;用于碱性矿石如球团样品中砷的分析,多名操作者的测定结果吻合。
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关键词:
- 砷 /
- 硫-磷混酸 /
- 银-二乙基二硫代氨基甲酸钠法(Ag—DDTC) /
- 样品溶解 /
- 铁矿石
Abstract: The sample dissolution method is improved through using mixed acid of sulfuric acid-phosphoric acid to dissolve iron ore samples. Arsenic in sample solution from the new sample dissolution method is then determined by Ag-DDTC method. The new method provid-
Key words:
- arsenic /
- sulfuric /
- acid-phosphoric /
- acid
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